Iron & Ammonium Citrate

SL. NO
TESTS
STANDARDS
1
Characters
A
Description
Thin, transparent, dark red scales or granules or a brownish red powder; odourless; deliquescent in moist air and is affected by light.
B
Solubility
Very soluble in water; practically insoluble in ethanol (95%).
2
Identification
A
Reaction of Ferric salts
i
Reaction A
An intense blue precipitate should be produced which should be insoluble in dilute hydrochloric acid.
ii
Reaction B
The red colour should disappear.
ii
Reaction C
A stable green colour should be formed.
B
Reaction of Citrates
i
Reaction A
A white precipitate should be formed which should be soluble in 6M acetic acid.
ii
Reaction B
A violet colour should be produced which should change to violet-blue.
3
Arsenic
Not more than 4 ppm.
4
Lead
Not more than 30 ppm.
5
Zinc
Not more than 50 ppm.
6
Free Ferric Compounds
No blue precipitate should be formed.
7
Chlorides
Not more than 0.25%
8
Sulphate
Not more than 0.3%
9
Assay
Between 20.5% and 22.5% (of iron, Fe)